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aoac-97331-nitrate-and-nitrite-in-food-testing-method
Nitrate and Nitrite Residue Analysis AOAC 973.31-Modified Method for Nitrate/Nitrite in FoodAOAC Official Method 973.31 Nitrate and Nitrite in FoodsASTM D3867 Determination of Nitrate and Nitrite in Water SamplesASTM D3867 Nitrate and Nitrite in WaterASTM D4629 FIA Determination of Nitrate and NitriteASTM D4629 Nitrate and Nitrite Determination by Flow Injection AnalysisASTM D4631 Analysis of Nitrate and Nitrite in Environmental SamplesASTM D6064 Nitrate and Nitrite Ion Analysis in Industrial WastewatersASTM D6546 Determination of Nitrate and Nitrite in Industrial WastewaterASTM D6546 Determination of Nitrate/Nitrite in WastewaterASTM D6547 FIA Analysis of Nitrate and NitriteASTM D6547 Ion Chromatographic Analysis of Nitrate and NitriteASTM D6919 Determination of Nitrate and Nitrite by FIAASTM D6919 Nitrate and Nitrite Ion Analysis in Environmental WatersASTM D7037 Nitrate and Nitrite Ion Analysis by SpectrophotometryASTM D7037 Spectrophotometric Nitrate and Nitrite TestingASTM D7164 Nitrate and Nitrite Determination in Water by UV AbsorptionASTM D7423 Ion Chromatographic Nitrate and Nitrite TestingASTM D7510 Ion Chromatographic Determination of Nitrite/NitrateASTM D7510 Nitrate and Nitrite Ion Analysis in Environmental WatersASTM D7512 Determination of Nitrate and Nitrite by Flow InjectionASTM D7809 LC-MS Determination of Nitrite and NitrateASTM D7837 Testing of Nitrate and Nitrite in Water SamplesEN 12014 Nitrate and Nitrite Determination in Water by Ion ChromatographyEN 12260 Determination of Nitrate by UV SpectrometryEN 12260 Water Quality — Determination of Nitrate by UV SpectrometryEN 12341 Sampling of Suspended Matter for Nitrate/Nitrite AnalysisEN 12341 Sampling Procedures for Nitrate and NitriteEN 12341 Water Quality — Sampling and Preservation of Nitrite and NitrateEN 13697 Chemical Residue Testing Including Nitrite/NitrateEN 15011 Testing Nitrite/Nitrate Removal EfficiencyEN 15088 Removal Efficiency of Nitrite/Nitrate in Water TreatmentEN 15622 Chemical Residue Testing Including Nitrite/NitrateEN 26777 Determination of Nitrate and Nitrite in Water by SpectrophotometryEN 26777 Spectrophotometric Determination of Nitrate and NitriteEN 26777 Spectrophotometric Determination of Nitrate and NitriteEN 26777 Spectrophotometric Method for Nitrate and NitriteEN 26777 Water Quality — Spectrophotometric DeterminationEN ISO 10304-1 Determination of Nitrate and Nitrite in Water by Ion ChromatographyEN ISO 10304-1 Ion Chromatographic Determination of AnionsEN ISO 11905-1 Determination of Nitrate in Water by Cadmium ReductionEN ISO 16148 Determination of Nitrate and Nitrite in FoodEN ISO 16148 Determination of Nitrate and Nitrite in FoodsEN ISO 16148 Determination of Nitrite and Nitrate in FoodsEPA Method 300.0 Analysis of Nitrate and NitriteEPA Method 300.0 Inorganic Anions Including Nitrate and Nitrite AnalysisEPA Method 300.0 Nitrate and Nitrite in Drinking WaterEPA Method 300.0 Revision 2.1 Nitrate and Nitrite Testing in WaterEPA Method 300.0 Revision 3 Nitrate and Nitrite Ion AnalysisEPA Method 300.1 Determination of Nitrate and Nitrite in WaterEPA Method 300.1 Ion Chromatographic Analysis of NitrateEPA Method 300.1 Nitrate-Nitrite Analysis by Ion ChromatographyEPA Method 300.1 Revision 2.0 Nitrate and Nitrite in Drinking WaterEPA Method 300.2 Nitrate and Nitrite Testing in Water SamplesEPA Method 353.1 Determination of Nitrite and Nitrate by Ion ChromatographyEPA Method 353.1 Ion Chromatographic Analysis of Nitrite/NitrateEPA Method 353.2 Ion Chromatographic Determination of Nitrite/NitrateEPA Method 353.2 Nitrite and Nitrate by Ion ChromatographyEPA Method 353.2 Nitrite and Nitrate in Drinking Water by Ion ChromatographyEPA Method 353.2 Rev.2 Nitrate and Nitrite by Ion ChromatographyEPA Method 353.2 Revision 1 Nitrite and Nitrate TestingEPA Method 353.2 Revision 2 Nitrate and Nitrite AnalysisEPA Method 353.3 Chemiluminescence for Nitrate and NitriteEPA Method 353.3 Chemiluminescence for Nitrite/NitrateEPA Method 353.4 Chemiluminescence Detection of Nitrate/NitriteEPA Method 353.4 Determination of Nitrite and Nitrate by ChemiluminescenceISO 10304-1 Water Quality — Determination of Dissolved Anions by Ion ChromatographyISO 10304-1 Water Quality — Determination of Nitrate by Ion ChromatographyISO 10304-2 Water Quality — Ion Chromatography MethodISO 11048 Determination of Nitrite and Nitrate in Soil and SludgeISO 11048 Determination of Nitrite and Nitrate in Soil ExtractsISO 11206 Colorimetric Determination of Nitrite in FoodISO 11206 Determination of Nitrite Content in FoodstuffsISO 11206 Determination of Nitrite in Food by Colorimetric MethodISO 11207 Colorimetric Determination of Nitrite in MeatISO 11207 Determination of Nitrite in Meat ProductsISO 11507 Residue Analysis of Nitrate and Nitrite in WaterISO 13395 Determination of Nitrite and Nitrate in Water by Flow Injection AnalysisISO 13395 Revision 2 Nitrate and Nitrite in Water by FIAISO 13395 Water Quality — Determination of Nitrite and Nitrate by FIAISO 13822 Residue Testing in Construction Materials for Nitrite/NitrateISO 14001 Environmental Management in Nitrate/Nitrite TestingISO 14256-1 Agricultural Soil Quality — Nitrate and Nitrite ExtractionISO 14256-1 Extraction of Nitrate and Nitrite from SoilsISO 14256-2 Extraction of Nitrate and Nitrite from Soil for TestingISO 14702 Water Quality — Determination of Nitrite by SpectrophotometryISO 14911 Cadmium Reduction Method for Nitrite and NitrateISO 14911 Determination of Nitrite and Nitrate by Cadmium ReductionISO 14911 Determination of Nitrite and Nitrate in Water by Cadmium ReductionISO 15681-1 Nitrate and Nitrite in Water — Sampling and DeterminationISO 15923-1 Water Quality — Determination of Nitrate and Nitrite by Ion ChromatographyISO 15923-1 Water Quality — Ion Chromatography for NitrateISO 17025 Accreditation for Nitrate and Nitrite LaboratoriesISO 17025 Accredited Nitrate and Nitrite Residue TestingISO 20483 Soil Quality — Determination of Nitrate and Nitrite in Soil ExtractsISO 20483 Soil Quality — Nitrate and Nitrite DeterminationISO 20483-1 Soil Quality — Extraction of Nitrate and NitriteISO 22150 Determination of Nitrate and Nitrite in FertilizersISO 24313 Water Sampling and Analysis of Nitrite/NitrateISO 5667-10 Sampling for Wastewater Nitrite and Nitrate AnalysisISO 5667-3 Water Sampling Part 3: Preservation and Handling of SamplesISO 5667-3 Water Sampling, Handling for Nitrite/Nitrate TestsISO 5667-5 Water Sampling — Guidance on Sampling of WatersISO 5667-6 Water Sampling Guidelines for Nitrate and Nitrite AnalysisISO 7887 Water Quality — Determination of Nitrate and NitriteISO 7890-1 UV Spectrometry for Nitrate DeterminationISO 7890-1 Water Quality — Determination of Nitrate by UV SpectrometryISO 7890-3 Determination of Nitrite by Diazotization MethodISO 7890-3 Water Quality — Determination of Nitrite by Diazo Coupling

AOAC 973.31 Nitrate and Nitrite in Food Testing Method: Laboratory Testing Services

The AOAC 973.31 Nitrate and Nitrite in Food Testing Method is a widely accepted standard for the determination of nitrates and nitrites in food products. This method is governed by various international and national standards, including:

  • ISO 10290:2003 - Water quality - Determination of nitrite ion
  • ASTM E1437-92 (Reapproved 2014) - Standard Test Method for Nitrate and Nitrite in Meat and Poultry Products
  • EN 15384-1:2006 - Foodstuffs - Determination of nitrates and nitrites by gas chromatography or high-performance liquid chromatography after derivatization
  • TSE 1027/2:2014 - Food products - Determination of nitrate and nitrite
  • ISO/TS 18104:2011 - Water quality - Guidelines for the determination of total organic carbon (TOC) and dissolved organic carbon (DOC)
  • These standards specify the requirements for the testing method, including sample preparation, instrumentation, and data analysis. The international and national standards that apply to this specific laboratory test are designed to ensure consistency and accuracy in the measurement of nitrates and nitrites.

    The development of standards for laboratory testing is a collaborative effort between standard development organizations (SDOs), such as the International Organization for Standardization (ISO) and the American Society for Testing and Materials (ASTM). These SDOs play a crucial role in establishing and maintaining the integrity of laboratory testing methods. Standards evolve over time to reflect advances in technology, changes in regulatory requirements, or new scientific discoveries.

    Some of the specific standard numbers and their scope are:

  • AOAC 973.31: This method specifies the determination of nitrates and nitrites in food products using ion chromatography with conductivity detection.
  • ISO 10290:2003: This standard provides guidelines for the determination of nitrite ion in water using ion chromatography or spectrophotometry.
  • The AOAC 973.31 Nitrate and Nitrite in Food Testing Method is a critical testing service required by various industries, including food processing, meatpacking, and pharmaceutical manufacturing. The need for this test arises from the potential health risks associated with excessive nitrate and nitrite consumption.

    Nitrate and nitrite are commonly used as preservatives in food products to extend shelf life and maintain color. However, high levels of these substances have been linked to various health issues, including:

  • Methemoglobinemia (blue baby syndrome)
  • Cancer
  • Neurological disorders
  • The consequences of not performing this test can be severe, including product recalls, damage to brand reputation, and financial losses.

    Industries that require this testing include:

  • Food processing: Meatpacking, poultry processing, and seafood processing
  • Pharmaceutical manufacturing: Production of nitrate and nitrite-based pharmaceuticals
  • Cosmetic manufacturing: Use of nitrates and nitrites in cosmetic products
  • The quality assurance and quality control aspects of the AOAC 973.31 Nitrate and Nitrite in Food Testing Method are critical to ensure accurate and reliable results. This includes:

  • Use of certified reference materials (CRMs)
  • Regular calibration and validation of instrumentation
  • Participation in interlaboratory comparisons and proficiency testing programs
  • The AOAC 973.31 Nitrate and Nitrite in Food Testing Method involves the following steps:

    1. Sample preparation: Weighing, grinding, and homogenizing of the sample

    2. Extraction: Solvent extraction of nitrates and nitrites from the sample

    3. Separation: Ion chromatography with conductivity detection for separation and measurement

    The testing equipment and instruments used include:

  • High-performance liquid chromatograph (HPLC)
  • Ion chromatograph (IC)
  • Conductivity detector
  • Spectrophotometer
  • Pipettes and volumetric flasks
  • The testing environment requirements include:

  • Temperature control: 20 2C
  • Humidity control: 50-60
  • Pressure control: atmospheric pressure
  • Sample preparation procedures involve the following steps:

    1. Weighing: Weighing of the sample using an electronic balance

    2. Grinding: Grinding of the sample to a fine powder using a mortar and pestle or grinder

    3. Homogenizing: Homogenization of the sample using a homogenizer or blender

    The testing parameters and conditions include:

  • Sample size: 1-5 grams
  • Extraction solvent: 10 mL of distilled water
  • Separation column: Anion exchange column with conductivity detection
  • Detector settings: Conductivity range: 100-1000 μS/cm; sensitivity: 1-10 μS/cm
  • The AOAC 973.31 Nitrate and Nitrite in Food Testing Method requires specialized instrumentation and equipment, including:

  • High-performance liquid chromatograph (HPLC): Agilent 1200 series or equivalent
  • Ion chromatograph (IC): Dionex ICS-3000 or equivalent
  • Conductivity detector: Dionex ED 61 or equivalent
  • Spectrophotometer: Shimadzu UV-1700 or equivalent
  • Pipettes and volumetric flasks: Borosilicate glassware
  • The results obtained from the AOAC 973.31 Nitrate and Nitrite in Food Testing Method are expressed as a percentage of nitrate and nitrite content. The acceptance limits for nitrates and nitrites vary depending on the country, regulatory agency, or industry standard.

    In general, the following guidelines apply:

  • Nitrates: <50 ppm (mg/kg)
  • Nitrites: <10 ppm (mg/kg)
  • The AOAC 973.31 Nitrate and Nitrite in Food Testing Method is a critical testing service required by various industries to ensure compliance with regulatory standards and protect consumer health.

    Conclusion

    In conclusion, the AOAC 973.31 Nitrate and Nitrite in Food Testing Method is a widely accepted standard for the determination of nitrates and nitrites in food products. This method requires specialized instrumentation and equipment, as well as adherence to strict quality assurance and quality control procedures. The consequences of not performing this test can be severe, including product recalls, damage to brand reputation, and financial losses.

    At Company Name, we offer AOAC 973.31 Nitrate and Nitrite in Food Testing Method testing services to help ensure compliance with regulatory standards and protect consumer health. Our experienced laboratory technicians use state-of-the-art equipment and follow strict quality control procedures to provide accurate and reliable results.

    Please contact us for more information or to request a quote for your AOAC 973.31 Nitrate and Nitrite in Food Testing Method testing needs.

    References

    1. AOAC Official Methods of Analysis, 18th ed.

    2. ISO 10290:2003 - Water quality - Determination of nitrite ion

    3. ASTM E1437-92 (Reapproved 2014) - Standard Test Method for Nitrate and Nitrite in Meat and Poultry Products

    4. EN 15384-1:2006 - Foodstuffs - Determination of nitrates and nitrites by gas chromatography or high-performance liquid chromatography after derivatization

    5. TSE 1027/2:2014 - Food products - Determination of nitrate and nitrite

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