EUROLAB
iso-11357-1-plastics-dsc-general-principles
Thermal Analysis ASTM D3418 Melting and Crystallization Temperature Measurement by DSCASTM D3418 Thermal Analysis of Polymers by DSCASTM D3895 Thermal Stability of Polymers by TGAASTM E1269 DSC Heat Flow Rate DeterminationASTM E1356 Differential Scanning Calorimetry (DSC) for PolymersASTM E1356 Differential Scanning Calorimetry of PharmaceuticalsASTM E1356 DSC of AdhesivesASTM E1356-08 DSC Glass Transition and Melting Point DeterminationASTM E1460 DSC of Composite MaterialsASTM E1461 Laser Flash Method for Thermal DiffusivityASTM E1462 Simultaneous Thermal Analysis of Polymer BlendsASTM E1545 DSC of FoodstuffsASTM E1582 Thermal Analysis of CoatingsASTM E1590 DMA Frequency Sweep TestASTM E1821 Temperature-Dependent Mechanical AnalysisASTM E1952 TGA of High-Temperature StabilityASTM E1959 TGA Analysis of Polymers Under Oxygen AtmosphereASTM E2001 Modulated DSC for Polymer CharacterizationASTM E2004 TGA of Composite MaterialsASTM E2041 Thermal Analysis of Battery MaterialsASTM E2072 TMA of MetalsASTM E2179 DMA Temperature Sweep TestASTM E2232 TMA for Coefficient of Thermal Expansion in MetalsASTM E2280 DSC for Thin Film MaterialsASTM E2297 Thermal Conductivity Measurement by TGAASTM E2429 Thermal Analysis of GlassASTM E2439 Thermogravimetric Analysis of Food ProductsASTM E2546 Measurement of Thermal Expansion by TMAASTM E2548 Simultaneous TGA and DSC AnalysisASTM E2549 Simultaneous TGA-FTIR for Decomposition Gas AnalysisASTM E2580 DMA of ElastomersASTM E2608 Thermal Analysis of Ceramic MaterialsASTM E2677 Thermal Analysis of Pharmaceutical PowdersASTM E2716 Dynamic Mechanical Analysis (DMA) of PolymersASTM E2719 DMA Creep and Recovery TestingASTM E2781 Temperature Modulated DSC for Complex Thermal EventsASTM E2782 Thermomechanical Analysis (TMA) of MaterialsASTM E2783 High-Temperature Thermal AnalysisASTM E344 Heat Capacity Measurements by DSCASTM E537 Thermomechanical Analysis for Dimensional ChangesASTM E968 Thermogravimetric Analysis (TGA) of MaterialsISO 11357-1 Adhesive Thermal PropertiesISO 11357-1 Composite Thermal AnalysisISO 11357-1 Food Thermal PropertiesISO 11357-1 Pharmaceutical Thermal AnalysisISO 11357-1 Pharmaceutical Thermal PropertiesISO 11357-1 Plastics — DSC General Testing ProceduresISO 11357-1 Thin Film Thermal CharacterizationISO 11357-2 Plastics — DSC Determination of Glass Transition TemperatureISO 11357-3 Plastics — DSC Crystallization ParametersISO 11357-3 Plastics — DSC Determination of Crystallization TemperatureISO 11357-3 Polymer Thermal PropertiesISO 11357-4 Plastics — DSC Determination of Heat CapacityISO 11357-4 Plastics — Heat Capacity MeasurementISO 11357-5 Plastics — DSC Determination of Oxidation Induction TimeISO 11357-6 Plastics — DSC Crystallinity MeasurementsISO 11358-1 Composite Thermal DecompositionISO 11358-1 Food Thermal Decomposition AnalysisISO 11358-1 Plastics — TGA General PrinciplesISO 11358-1 Thermal Stability TestingISO 11358-2 Plastics — TGA Decomposition ProfilesISO 11358-2 Polymer Thermal DegradationISO 11358-3 Plastics — TGA Thermal StabilityISO 11358-4 Plastics — TGA with Gas AnalysisISO 11359-2 Metal Thermal ExpansionISO 11359-2 Metals — TMA Expansion TestingISO 11359-2 Plastics — TMA Determination of Coefficient of Thermal ExpansionISO 11359-3 Plastics — TMA Linear Thermal ExpansionISO 11359-3 Thermal Expansion TestingISO 15911 Coating Thermal BehaviorISO 18246 Battery Material Thermal TestingISO 18927-1 Ceramic Thermal TestingISO 22007-2 Plastics — Thermal Conductivity TestingISO 22007-4 Plastics — Thermal DiffusivityISO 6721-1 Elastomer Dynamic Mechanical TestingISO 6721-1 Plastics — DMA General PrinciplesISO 6721-10 Plastics — DMA Frequency SweepISO 6721-11 Plastics — DMA Creep and Stress RelaxationISO 6721-2 Plastics — DMA Tensile ModeISO 6721-7 Plastics — DMA Temperature SweepISO 7219 Glass Thermal Properties

ISO 11357-1 Plastics DSC General Principles Laboratory Testing Service: A Comprehensive Guide

ISO 11357-1 is a widely recognized international standard for the testing of plastics using Differential Scanning Calorimetry (DSC). This standard provides a framework for laboratories to perform accurate and reliable DSC tests on plastic materials. The standard is developed by the International Organization for Standardization (ISO) and is available in multiple languages.

International Standards Governing ISO 11357-1 Testing

  • ISO 11357-1:2016(E) - Plastics Differential scanning calorimetry (DSC) Part 1: General principles
  • ASTM D3418-08(2020)e1 - Standard Test Method for Heat of Combustion of Liquid Hydrocarbon Fuels by Bomb Calorimeter
  • EN ISO 11357-1:2016 - Plastics Differential scanning calorimetry (DSC) Part 1: General principles
  • TSE EN ISO 11357-1:2017 - Plastics Differential scanning calorimetry (DSC) Part 1: General principles
  • Standard Development Organizations and Their Role

    The International Organization for Standardization (ISO) is responsible for developing and maintaining the ISO 11357-1 standard. The ISO has a global network of member bodies that contribute to the development and approval of standards.

    How Standards Evolve and Get Updated

    Standards are regularly reviewed and updated to reflect changes in technology, industry practices, and regulatory requirements. The process involves a thorough review of existing standards, consultation with stakeholders, and testing by laboratories.

    Standard Compliance Requirements for Different Industries

    ISO 11357-1 is widely used across various industries, including plastics manufacturing, chemical processing, automotive, aerospace, and consumer goods. Compliance with this standard is often mandatory or recommended for regulatory purposes, product safety, and quality assurance.

    Consequences of Not Performing ISO 11357-1 Testing

    Failure to perform DSC testing on plastic materials can lead to:

  • Inaccurate material properties
  • Reduced product performance and reliability
  • Non-compliance with regulatory requirements
  • Potential safety risks
  • Industries and Sectors that Require ISO 11357-1 Testing

    ISO 11357-1 is commonly used in the following industries:

  • Plastics manufacturing
  • Chemical processing
  • Automotive
  • Aerospace
  • Consumer goods
  • Pharmaceutical industry
  • Risk Factors and Safety Implications

    DSC testing of plastic materials can help identify potential risks, such as:

  • Thermal degradation
  • Material instability
  • Potential for ignition or combustion
  • Impact on product performance and reliability
  • Quality Assurance and Quality Control Aspects

    ISO 11357-1 testing involves rigorous quality assurance and control measures to ensure accurate results. These include:

  • Calibration of equipment
  • Validation of methods
  • Sample preparation and handling procedures
  • Data analysis and interpretation
  • Step-by-Step Explanation of DSC Testing

    DSC testing involves the following steps:

    1. Equipment calibration

    2. Sample preparation

    3. Heating and cooling cycles

    4. Data collection and analysis

    Testing Equipment and Instruments Used

  • Differential scanning calorimeter (DSC)
  • Thermocouples
  • Temperature control systems
  • Data acquisition software
  • Testing Environment Requirements

    The testing environment should be:

  • Controlled temperature ( typically between -150C to 600C)
  • Stable humidity level (less than 60)
  • Limited vibrations and noise levels
  • Sample Preparation Procedures

    Samples for DSC testing are typically prepared as follows:

  • Cutting or grinding the sample
  • Weighing and measuring the sample
  • Sealing the sample in an aluminum pan
  • Testing Parameters and Conditions

    The following parameters are typically used during DSC testing:

  • Temperature range (typically between -150C to 600C)
  • Heating rate (typically between 5C/min to 20C/min)
  • Cooling rate (typically between 5C/min to 20C/min)
  • Measurement and Analysis Methods

    Data analysis involves the following steps:

    1. Plotting of thermograms

    2. Calculation of thermal properties (e.g., melting point, glass transition temperature)

    3. Data validation and verification

    Calibration and Validation Procedures

    The DSC equipment is calibrated using a certified standard material. The calibration procedure involves the following steps:

  • Calibration of the temperature control system
  • Verification of the DSC instrument accuracy
  • Interpretation of Test Results

    DSC test results are interpreted based on the following factors:

  • Thermal properties (e.g., melting point, glass transition temperature)
  • Material stability and degradation behavior
  • Potential for thermal runaway or ignition
  • Certification and Accreditation Aspects

    ISO 11357-1 testing is performed by accredited laboratories that have undergone rigorous quality management system audits. The laboratory certification process involves:

  • ISO/IEC 17025 accreditation
  • NIST traceability
  • Quality management system implementation
  • Data Analysis and Interpretation Software

    The following software packages are commonly used for data analysis and interpretation:

  • TA Instruments Universal Analysis software
  • Mettler Toledos STAR software
  • PerkinElmers Pyris software
  • Need help or have a question?
    Contact us for prompt assistance and solutions.

    Latest News

    View all

    JOIN US
    Want to make a difference?

    Careers