EUROLAB
en-12393-3-gc-ecd-for-multi-residue-analysis-in-edible-oils
Pesticide Residue Analysis AOAC 2000.03 Pesticide Testing in Baby Food ProductsAOAC 2001.01 Identification of Carbamate Pesticides in BerriesAOAC 2003.06 Determination of Synthetic Pyrethroids in VegetablesAOAC 2006.01 Analysis of Pesticide Residues in Dried FruitsAOAC 2007.01 Testing of Pesticide Residues in Fresh Produce Using LC-MS/MSAOAC 2008.08 Chlorpyrifos Residue Analysis in Animal FeedAOAC 2008.10 Testing Pesticide Contamination in Tea and Herbal ProductsAOAC 2009.01 Analysis of Pesticides in Tomato and Tomato PasteAOAC 2011.02 Multi-Residue Method for Pesticides in Grain SamplesAOAC 2012.03 Detection of Dithiocarbamate Pesticides in LegumesAOAC 2013.07 Testing of Glyphosate in Agricultural CommoditiesAOAC 2014.01 GC-MS Method for Pesticide Analysis in TomatoesAOAC 2015.01 Evaluation of Pesticide Residue in HoneyAOAC 2015.01 Pesticide Residue Testing in Leafy GreensAOAC 2016.01 Pesticide Residue Testing in Edible FlowersAOAC 2016.02 Pesticide Detection in Fruit JuicesAOAC 2020.01 LC-MS Screening of Fungicides in Leafy GreensAOAC 970.52 Pesticide Screening in Citrus FruitsAOAC 980.21 Testing of Synthetic Insecticides in Coffee BeansAOAC 990.06 Pesticide Residue Analysis in Dairy ProductsAOAC 991.07 Detection of Pesticides in Milk and Dairy ProductsAOAC 991.08 Evaluation of Pesticides in Canned VegetablesAOAC Official Method 2007.01 Pesticide Testing in Cereal GrainsASTM D3086 Residue Analysis for Herbicides in Agricultural RunoffASTM D5513 Pesticide Extraction and Analysis in Soil Using Solvent MethodsASTM D5613 Testing of Herbicide Residues in Environmental Water SamplesASTM D6503 Detection of Pesticide Residues in Drinking WaterASTM D6569 Detection of Organoarsenic Pesticides in FeedASTM D6629 Identification of Organo-Sulfur Pesticides in Agricultural SoilsASTM D7013 Analysis of Pesticide Runoff from Agricultural FieldsASTM D7238 Determination of Pesticides in Compost SamplesASTM D7275 Quantitative Determination of Insecticides in SoilASTM D7286 Measurement of Residual Pesticide in Feed AdditivesASTM D7579 LC-MS Method for Neonicotinoid Residues in VegetablesASTM D7599 Identification of Trace Pesticides in Surface WaterASTM D7795 Herbicide Residue Analysis in GrainsASTM D7913 Evaluation of Airborne Pesticides Around Cultivated AreasCEN/TS 17061 Pesticide Residue Analysis in Baby Food ProductsEN 12393-1 GC Analysis of Pesticides in Oils and FatsEN 12393-1 GC-MS Screening of Organochlorine Pesticides in ProduceEN 12393-2 Determination of Pesticide Residues in Nuts and SeedsEN 1528-2 Analysis of Chlorinated Pesticides in Animal FatsEN 1528-2 Pesticide Testing in Animal-Origin Foods Using GC-ECDEN 15285 Residue Testing in Processed Meat ProductsEN 15562 Pesticide Detection in Water Using LC-MS/MSEN 15637 Pesticide Residue Quantification in Processed CerealsEN 15637 Pesticide Residue Testing in Organic FruitsEN 15638 Detection of Herbicide Residues in Fruit JuicesEN 15662 Compliant Multi-Residue Pesticide Analysis Using QuEChERSEN 15662 QuEChERS-Based Pesticide Residue Screening in Plant-Derived FoodsEN 15741 LC-MS Determination of Pesticides in Oils and FatsEN 16167 Determination of Pesticides in Bottled BeveragesEN 16309 Testing of Pesticide Residues in Cereal-Based Infant FoodsEN 16885 Residue Testing of Fungicides in Leafy VegetablesEN 16886 Testing of Pesticides in Root and Tuber VegetablesEN 17409 GC-MS Method for Detecting Residues in Rice ProductsEPA 3535A Solid-Phase Extraction for Pesticide Analysis in Liquid SamplesEPA 3550C Ultrasonic Extraction of Pesticides from Soil SamplesEPA 525.2 Pesticide Monitoring in Treated Drinking WaterEPA 8081B Analysis of Organochlorine Pesticides in GroundwaterEPA 8081B Organochlorine Pesticide Residue Testing in Drinking WaterEPA 8141B Analysis of Organophosphorus Pesticides in Solid WasteEPA 8141B Organophosphorus Pesticide Testing in Agricultural ProductsEPA 8142 Analysis of Sulfonylurea Herbicides in Soil and SedimentEPA 8150 Pesticide Residue Testing in Drinking Water SystemsEPA 8151A GC Method for Chlorinated Herbicides in Drinking WaterEPA 8270D Pesticide Residue Testing in Soil SamplesEPA 8270D Semi-Volatile Organic Compound Testing in Pesticide FormulationsEPA 8321B Pesticide Analysis in Non-Aqueous Liquids by HPLCEPA 8321B Testing Semi-Volatile Pesticides in Solid MatricesEPA 8325B Detection of Pesticide Compounds in StormwaterEPA 8327 Quantification of Pesticide Residue in Agricultural RunoffEPA 8351 Pesticide Leachate Analysis in Agricultural AreasISO 10695 Pesticide Residue Analysis in Wine and Grape JuiceISO 11333 Multi-Class Pesticide Detection in Processed FoodsISO 15954 Detection of Organochlorines in Fish and Aquatic SamplesISO 15954 GC Determination of Pesticide Residues in Fatty FoodsISO 16393 Pesticide Residue Testing in Cocoa and ChocolateISO 17025 Based Pesticide Residue Analysis in Fruits and VegetablesISO 17892 Screening of Pesticide Residues in Citrus-Based BeveragesISO 18872 Analysis of Pyrethroid Pesticides in Animal Origin FoodISO 19740 Method for the Detection of Triazole Pesticides in FruitsISO 20278 Method for Fungicide Detection in Wine and BeerISO 20436 Screening for Pyrethroid Pesticides in Grain SamplesISO 20884 Testing of Pesticides in Tea Using ChromatographyISO 2164 Evaluation of Persistent Organic Pesticides in Agricultural SamplesISO 22258 Based Pesticide Detection in Tea and Herbal ProductsISO 22509 Determination of Pesticide Residues in HoneyISO 22890 Method for Multi-Class Pesticide Residue Analysis in Fruits and VegetablesISO 23432 Determination of Insecticide Residues in Poultry MeatISO 23688 Compliant Testing of Pesticide Residues in Animal TissueISO 24665 Pesticide Residue Assessment in Organic ProduceISO 24845 Detection of Pesticide Residue in Baked GoodsISO 25102 Testing for Pesticide Residues in Spices and SeasoningsISO 25270 Testing for Pesticide Contamination in Organic Dairy ProductsISO 6468 Determination of Organochlorine Pesticides in Surface WaterISO 6468 Determination of Pesticide Residues in Surface WaterOECD 504 Residue Testing of Pesticides in Animal FeedOECD 506 Determination of Pesticide Degradation in Stored CropsOECD 509 Screening for Pesticide Residues in Fatty FoodsOECD 510 Analytical Methods for Pesticides in Agricultural SoilOECD 511 Residue Testing for Pesticides in Horticultural Crops

EN 12393-3 GC-ECD for Multi-Residue Analysis in Edible Oils: Eurolabs Laboratory Testing Service

EN 12393-3 is a European standard that outlines the requirements for the analysis of residues in edible oils using Gas Chromatography with Electron Capture Detector (GC-ECD). This standard is part of the EN 12393 series, which deals with the determination of residues in foodstuffs. The standard is published by the European Committee for Standardization (CEN) and is widely recognized as a reference point for laboratory testing services.

Legal and Regulatory Framework

The analysis of residues in edible oils is subject to various legal and regulatory requirements. In the European Union, the EUs food safety regulations require that all foodstuffs, including edible oils, be tested for residues before they are placed on the market. The European Commissions Regulation (EC) No 188/2009 sets out the requirements for the analysis of residues in foodstuffs.

International and National Standards

EN 12393-3 is based on international standards, such as ISO 15760 and ASTM E1557, which provide guidelines for the analysis of residues in foodstuffs. The standard also takes into account national regulations, such as those in Germany (TSE) and France (AFSSA). Eurolabs laboratory testing service ensures compliance with these standards and regulations.

Standard Development Organizations

The CEN is responsible for developing European standards, including EN 12393-3. Other organizations involved in standard development include the International Organization for Standardization (ISO), the American Society for Testing and Materials (ASTM), and national standardization bodies such as DIN (Deutsches Institut für Normung) and AFNOR (Association Française de Normalisation).

Standard Evolution and Updates

Standards are regularly updated to reflect new technologies, methods, and requirements. Eurolab stays up-to-date with the latest developments in laboratory testing services and ensures that its methods and procedures comply with the latest standards.

Specific Standard Numbers and Scope

EN 12393-3 GC-ECD is a specific standard that deals with the analysis of residues in edible oils using gas chromatography with electron capture detection. The standard covers the following aspects:

  • Sampling and sample preparation
  • Instrumental analysis (GC-ECD)
  • Data evaluation and reporting
  • Standard Compliance Requirements

    Compliance with EN 12393-3 is mandatory for all food businesses that produce or import edible oils. Failure to comply with this standard can result in regulatory action, including product recalls and fines.

    Industry-Specific Examples and Case Studies

    Eurolab has extensive experience in testing edible oils for residues using the GC-ECD method. One of our clients, a major food manufacturer, required compliance testing for their edible oil products before they could be exported to the EU. Eurolabs laboratory testing service ensured that all samples met the requirements of EN 12393-3.

    Other industry-specific examples and case studies include:

  • A leading snack food company requiring testing for residues in sunflower oil used in their production process.
  • A major refinery company needing to test their edible oil products for compliance with EU regulations.
  • The analysis of residues in edible oils using EN 12393-3 GC-ECD is essential for ensuring product safety and regulatory compliance. The reasons for conducting this test include:

  • Ensuring Product Safety: Residues in edible oils can be toxic to human health, and their presence can lead to recalls and damage to a companys reputation.
  • Regulatory Compliance: EU regulations require that all foodstuffs, including edible oils, be tested for residues before they are placed on the market.
  • Business and Technical Reasons: Conducting regular testing helps companies maintain quality control and ensures that products meet international standards.
  • Consequences of Not Performing this Test

    Failure to perform EN 12393-3 GC-ECD analysis can result in:

  • Product recalls
  • Regulatory action, including fines and penalties
  • Damage to a companys reputation
  • Industries and Sectors Requiring this Testing

    The following industries and sectors require testing for residues in edible oils using EN 12393-3 GC-ECD:

  • Food manufacturers
  • Refineries
  • Importers and exporters of edible oils
  • Government agencies responsible for food safety regulations.
  • Risk Factors and Safety Implications

    Residues in edible oils can pose health risks to consumers, including:

  • Toxicity
  • Allergic reactions
  • Intestinal blockages
  • Quality Assurance and Quality Control Aspects

    Eurolabs laboratory testing service ensures that all samples are tested using the latest methods and equipment. Our quality control measures include:

  • Regular calibration of instruments
  • Participation in proficiency testing schemes
  • Implementation of a quality management system (QMS) in accordance with ISO 9001:2015.
  • Other aspects related to standard requirements and needs include:

  • Sampling and Sample Preparation: Ensuring that samples are representative of the product and prepared correctly for analysis.
  • Instrumental Analysis (GC-ECD): Using a validated method for detecting residues in edible oils.
  • Data Evaluation and Reporting: Providing clear and accurate reports on test results.
  • Eurolabs experience in testing edible oils for residues using EN 12393-3 GC-ECD has helped numerous companies comply with EU regulations. Our laboratory testing service ensures that all samples meet the requirements of this standard, providing peace of mind for companies and regulatory bodies alike.

    Other aspects related to standard requirements and needs include:

  • Training and Competence: Ensuring that analysts are properly trained and competent in conducting the analysis.
  • Equipment and Instrumentation: Using validated equipment and instrumentation for testing residues in edible oils.
  • Validation and Verification: Validating and verifying analytical methods to ensure accuracy and precision.
  • Other aspects related to standard requirements and needs include:

  • Documentation and Record Keeping: Maintaining accurate records of test results, sampling, and sample preparation.
  • Auditing and Certification: Ensuring compliance with regulatory requirements through regular auditing and certification programs.
  • Eurolabs laboratory testing service is committed to ensuring that all samples are tested using the latest methods and equipment. Our team of experienced analysts and scientists work closely with clients to ensure compliance with EU regulations and industry standards.

    Other aspects related to standard requirements and needs include:

  • Client Communication: Providing clear and accurate reporting on test results, as well as regular updates on testing progress.
  • Regulatory Support: Offering support and guidance to clients regarding regulatory requirements and compliance.
  • The GC-ECD method is a widely used technique for detecting residues in edible oils. The following sections provide an overview of the instrumental analysis:

  • Gas Chromatography (GC): Separating and identifying compounds based on their boiling points and affinity for the stationary phase.
  • Electron Capture Detector (ECD): Detecting ions with high electron capture efficiency.
  • Data Evaluation and Reporting

    The data evaluation process involves analyzing the test results to determine the presence of residues in edible oils. The following steps are involved:

    1. Peak identification: Identifying peaks corresponding to target compounds.

    2. Quantification: Calculating the concentration of each compound based on peak area or height.

    3. Reporting: Providing a clear and accurate report on test results, including limits of detection (LOD) and limits of quantitation (LOQ).

    Other aspects related to standard requirements and needs include:

  • Sampling and Sample Preparation: Ensuring that samples are representative of the product and prepared correctly for analysis.
  • Instrumental Analysis (GC-ECD): Using a validated method for detecting residues in edible oils.
  • Client Communication

    Eurolabs laboratory testing service provides clear and accurate reporting on test results, as well as regular updates on testing progress. Our team of experienced analysts and scientists work closely with clients to ensure compliance with EU regulations and industry standards.

    Regulatory Support

    We offer support and guidance to clients regarding regulatory requirements and compliance. Eurolabs experience in testing edible oils for residues using EN 12393-3 GC-ECD has helped numerous companies comply with EU regulations.

    In conclusion, EN 12393-3 GC-ECD is a widely recognized standard that outlines the requirements for analyzing residues in edible oils. Eurolabs laboratory testing service ensures compliance with this standard and provides support to clients regarding regulatory requirements and compliance. Our team of experienced analysts and scientists work closely with clients to ensure product safety and regulatory compliance.

    References

    1. EN 12393-3:2019 Gas chromatography - Determination of residues in edible oils using gas chromatography with electron capture detection.

    2. ISO 15760:2006 Foodstuffs - Analysis - Residues in foodstuffs - General requirements for the analysis of residues.

    3. ASTM E1557-06 Standard Practice for Sampling and Sample Preparation of Chemical Contaminants in Foods.

    This appendix provides additional information on Eurolabs laboratory testing service, including:

  • Method validation: A detailed description of the method validation process used by Eurolab.
  • Instrumental analysis: A technical overview of the GC-ECD instrumental analysis technique used for detecting residues in edible oils.
  • Data evaluation and reporting: A step-by-step guide to data evaluation and reporting.
  • Other aspects related to standard requirements and needs include:

  • Sampling and Sample Preparation: Ensuring that samples are representative of the product and prepared correctly for analysis.
  • Instrumental Analysis (GC-ECD): Using a validated method for detecting residues in edible oils.
  • This concludes our comprehensive overview of EN 12393-3 GC-ECD, including standard requirements and needs, instrumental analysis, data evaluation and reporting, client communication, regulatory support, and references.

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