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codex-gl-71-sampling-for-determination-of-pesticide-residues
Pesticide & Veterinary Drug Residues AOAC 2003.06 Chloramphenicol residue analysis in honeyAOAC 2004.08 Hormone residue detection in eggsAOAC 2006.03 Quantitation of residues in dairy productsAOAC 2007.01 Pesticide residue analysis in fruits and vegetables by LC-MS/MSAOAC 2008.05 Veterinary residue analysis in milk powderAOAC 2009.01 Pesticide residues in cocoa and chocolateAOAC 2010.01 Multiresidue analysis of pesticides in baby foodAOAC 2011.23 LC-MS/MS determination of sulfonamides in meatAOAC 2014.10 Tetracycline residues in fish and shellfish by ELISAAOAC 2015.06 Detection of pesticide residues in honey and bee productsAOAC 2016.04 Veterinary drug testing in poultry productsAOAC 2016.09 Veterinary drugs in seafood samplesAOAC 2017.02 Fluoroquinolone residue detection in beefAOAC 2017.09 Pesticide residues in citrus fruitsAOAC 2018.03 Veterinary drug residues in milk by LC-MS/MSAOAC 2018.09 Detection of macrolides in pork and beefAOAC 2019.02 Detection of β-lactam antibiotics in bovine milkAOAC 2020.04 LC-MS analysis of antiparasitics in sheep meatAOAC 2020.05 Multi-class pesticide screening in tea leavesAOAC 2021.06 Veterinary residues in dried meat productsAOAC 2022.01 Carbamate detection in vegetablesAOAC 2023.02 Veterinary drug screening in animal fatCAC/MRL 01 Maximum Residue Limits of Pesticides in Food Products TestingCodex CAC/MRL 1 Establishing pesticide MRLs in cereals and grainsCodex CXG 71-2009 Guidelines on residue monitoring programsCodex GL 56 Guidelines on Good Laboratory Practice for Pesticide Residue AnalysisCodex GL 56 Guidelines on performance criteria for methods of analysis for pesticidesCodex GL 81 Good laboratory practices for pesticide residue testingCodex GL 90 Guideline levels for residues of veterinary drugs in foodCodex MRL Database Reference MRLs for pesticide-veterinary crossoverEPA 1657 Determination of pesticide metabolites in cropsEPA 3052 Determination of heavy metals in fertilizers and feed via acid digestionEPA 310.1 Herbicide detection in plant-based samplesEPA 314.1 Pesticide testing in animal urine samplesEPA 40 CFR Part 180 Analysis of Tolerances for Pesticide Chemical ResiduesEPA 5035A Sample preservation for volatile pesticide residue testingEPA 507 Pesticide analysis in drinking water and juicesEPA 535 Determination of chloroacetanilide herbicides in produceEPA 549.2 Aldicarb and related pesticide testing in plant tissueEPA 551.1 Determination of volatile pesticide residues in vegetablesEPA 6010D Trace metals in feed samples for pesticide contaminationEPA 608.3 Detection of pesticides in fat-rich animal tissuesEPA 8000C General protocols for pesticide residue identificationEPA 8081B Organochlorine pesticide detection by gas chromatographyEPA 8141B Organophosphorus pesticides in food matricesEPA 8151A Herbicide testing in soil and agricultural produceEPA 8151B LC-MS/MS testing of veterinary pesticide synergy effectsEPA 8270E Determination of semi-volatile pesticide residues in foodEPA 8321B Analysis of polar pesticides in animal tissues by HPLC-MSEPA 8325B Emerging pesticide residues in herbal medicinesEPA 8327 LC-MS analysis of pesticide degradation products in meatEPA 8330A Analysis of nitroaromatic pesticide residues in grainEU 2002/657/EC Validation of analytical methods for veterinary drug residuesEU 2005/34/EC Identification of residues in fresh meatEU 2009/128/EC Sustainable use of pesticides in food safety testingEU 2018/782 Residue control plan for animal-based food productsEU 2021/601 Monitoring of pesticide residues in organic foodEU 2022/617 Harmonization of veterinary residue testing protocolsEU 37/2010 Annex II Veterinary medicine residue validationEU 37/2010 Veterinary drug residue limits in foodstuffs of animal originEU 396/2005 Compliance Testing for Pesticide Residues in Fruits and VegetablesEU 396/2005 Harmonized limits for pesticide residues in food and feedEU 396/2005 Maximum residue limits of pesticides in agricultural products testingEU 625/2017 Compliance testing of veterinary drugs in aquacultureEU 744/2004 Residue control measures in aquacultureEU 96/23/EC Monitoring substances in live animals and animal productsEU SANTE/11813/2017 Sampling procedures for pesticide testingEU SANTE/12682/2019 Pesticide residues determination by QuEChERS methodEU SANTE/2020/12830 Confirmatory methods for residue analysisFAO/WHO Manual of Pesticide Residue Analysis in Agricultural CommoditiesISO 13395 Nitrite/nitrate detection in vegetables and fruitsISO 15662 Pesticide residue screening using modified QuEChERSISO 15952 Pesticide residue testing in animal feedingstuffsISO 17094 Multiclass pesticide residue testing in oilseedsISO 17190 Detection of residues in fermented animal feedISO 18330 Pesticide and veterinary drug residue detection in herbsISO 18385 Measurement of pesticide residue cross-contaminationISO 1842 Analysis of pesticide residues in feed raw materialsISO 18512 Pesticide and antibiotic residues in animal dungISO 20418 Veterinary antibiotic residues in bovine serumISO 21010 Rapid screening for multi-class residues in animal tissueISO 21458 Screening of pesticide residues using multi-residue methodsISO 22855 Determination of pesticide degradation products in foodISO 22866 Determination of Spray Drift in Field Conditions for Pesticide ApplicationISO 22892 Analysis of persistent organic pollutants in livestockISO 23161 Screening of veterinary drug residues in eggsISO 23690 Determination of pesticide metabolites in animal feedISO 24662 Pesticide residue analysis in dried plant materialsISO 24687 Pesticide metabolite residue determination in poultryISO 25102 Multiresidue pesticide testing in spices and condimentsISO 6468 Pesticide residue analysis in water using liquid-liquid extractionJECFA Evaluation-Based Testing of Veterinary Drug Residues in Animal ProductsJECFA Pesticide residue risk evaluation for animal-derived productsJECFA Residue analysis of growth promoters in animal tissuesJECFA Residue evaluation of antibiotics in livestockJECFA Residue evaluation of veterinary drugs in cattle and poultryJECFA Residue limit setting for antimicrobials in livestockJECFA Risk assessment methodology for pesticide residue evaluationJECFA Risk-based residue evaluation for export commoditiesOECD TG 509 Residue Studies in Livestock for Veterinary Drugs DetectionSANCO/12495/2011 Method Validation for Pesticide Residue Analysis in FoodsVICH GL49 Risk Assessment Studies for Veterinary Medicinal Product Residues

Comprehensive Guide to Codex GL 71 Sampling for Determination of Pesticide Residues Testing Services

Provided by Eurolab: A Leading Laboratory Testing Service Provider

Codex GL 71 Sampling for determination of pesticide residues is a critical laboratory testing service that ensures the safety and quality of food products. This comprehensive guide will provide an in-depth overview of the relevant standards, regulations, and industry requirements governing this testing service.

International Standards

The Codex Alimentarius Commission (CAC) is responsible for developing international food standards, including those related to pesticide residues. The CAC has established a framework for evaluating pesticide residues on foods, which includes guidelines for sampling and analysis.

ISO 5725:2002(E) - Accuracy (trueness and precision) of measurement methods and results

This standard provides general principles and rules for the determination of accuracy (trueness and precision) of measurement methods and results. It is widely accepted as a reference document for laboratory testing services, including pesticide residue analysis.

ASTM D1068-17 - Standard Practice for Sampling Water from Wells

This standard outlines the procedures for sampling water from wells, which can be applied to other types of samples, such as food products, in certain situations.

National and Industry Standards

National and industry standards play a crucial role in ensuring compliance with regulatory requirements. For example:

TSE 1422:2018 - Foodstuffs - Pesticide residues - Determination of residues in food

This standard outlines the procedures for determining pesticide residues on food products, including sampling, preparation, and analysis.

EN ISO 14592:2009 - Water quality - Determination of water quality parameters - Sampling

This standard provides general guidelines for sampling water quality parameters, which can be applied to other types of samples in certain situations.

Standard Development Organizations

Standard development organizations (SDOs) are responsible for creating and maintaining industry standards. Some notable SDOs include:

  • International Organization for Standardization (ISO)

  • American Society for Testing and Materials (ASTM)

  • European Committee for Standardization (CEN)

    • These SDOs work closely with regulatory agencies, industries, and experts to develop and update standards that meet evolving needs.

    Evolution of Standards

    Standards evolve over time as new technologies emerge, scientific knowledge advances, or market requirements change. SDOs regularly review and update existing standards to ensure they remain relevant and effective.

    Example:

  • ISO 5725:2002(E) was revised in 2018 (ISO 5725-1:2018) to reflect the latest developments in measurement accuracy.

  • ASTM D1068-17 was updated from its previous version (ASTM D1068-12a) to incorporate new sampling techniques.

    • Industry-Specific Standards

    Standards can be specific to industries or sectors. For example:

  • In the food industry, standards like TSE 1422:2018 and EN ISO 14592:2009 are crucial for ensuring compliance with regulatory requirements.

  • In the water sector, standards like ASTM D1068-17 and EN ISO 14592:2009 provide guidance on sampling techniques.

    • Compliance Requirements

    Compliance with industry standards is essential for laboratories providing Codex GL 71 Sampling for determination of pesticide residues testing services. Failure to comply can result in:

  • Loss of accreditation or certification

  • Non-compliance with regulatory requirements

  • Damage to reputation and credibility

  • Financial penalties

    • To ensure compliance, laboratories must:

  • Follow established procedures for sampling and analysis

  • Use certified reference materials (CRMs) and internal quality control samples

  • Regularly review and update their quality management systems

  • Maintain accurate records of sampling, preparation, and analysis

    • Need help or have a question?
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