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iso-15952-pesticide-residue-testing-in-animal-feedingstuffs
Pesticide & Veterinary Drug Residues AOAC 2003.06 Chloramphenicol residue analysis in honeyAOAC 2004.08 Hormone residue detection in eggsAOAC 2006.03 Quantitation of residues in dairy productsAOAC 2007.01 Pesticide residue analysis in fruits and vegetables by LC-MS/MSAOAC 2008.05 Veterinary residue analysis in milk powderAOAC 2009.01 Pesticide residues in cocoa and chocolateAOAC 2010.01 Multiresidue analysis of pesticides in baby foodAOAC 2011.23 LC-MS/MS determination of sulfonamides in meatAOAC 2014.10 Tetracycline residues in fish and shellfish by ELISAAOAC 2015.06 Detection of pesticide residues in honey and bee productsAOAC 2016.04 Veterinary drug testing in poultry productsAOAC 2016.09 Veterinary drugs in seafood samplesAOAC 2017.02 Fluoroquinolone residue detection in beefAOAC 2017.09 Pesticide residues in citrus fruitsAOAC 2018.03 Veterinary drug residues in milk by LC-MS/MSAOAC 2018.09 Detection of macrolides in pork and beefAOAC 2019.02 Detection of β-lactam antibiotics in bovine milkAOAC 2020.04 LC-MS analysis of antiparasitics in sheep meatAOAC 2020.05 Multi-class pesticide screening in tea leavesAOAC 2021.06 Veterinary residues in dried meat productsAOAC 2022.01 Carbamate detection in vegetablesAOAC 2023.02 Veterinary drug screening in animal fatCAC/MRL 01 Maximum Residue Limits of Pesticides in Food Products TestingCodex CAC/MRL 1 Establishing pesticide MRLs in cereals and grainsCodex CXG 71-2009 Guidelines on residue monitoring programsCodex GL 56 Guidelines on Good Laboratory Practice for Pesticide Residue AnalysisCodex GL 56 Guidelines on performance criteria for methods of analysis for pesticidesCodex GL 71 Sampling for determination of pesticide residuesCodex GL 81 Good laboratory practices for pesticide residue testingCodex GL 90 Guideline levels for residues of veterinary drugs in foodCodex MRL Database Reference MRLs for pesticide-veterinary crossoverEPA 1657 Determination of pesticide metabolites in cropsEPA 3052 Determination of heavy metals in fertilizers and feed via acid digestionEPA 310.1 Herbicide detection in plant-based samplesEPA 314.1 Pesticide testing in animal urine samplesEPA 40 CFR Part 180 Analysis of Tolerances for Pesticide Chemical ResiduesEPA 5035A Sample preservation for volatile pesticide residue testingEPA 507 Pesticide analysis in drinking water and juicesEPA 535 Determination of chloroacetanilide herbicides in produceEPA 549.2 Aldicarb and related pesticide testing in plant tissueEPA 551.1 Determination of volatile pesticide residues in vegetablesEPA 6010D Trace metals in feed samples for pesticide contaminationEPA 608.3 Detection of pesticides in fat-rich animal tissuesEPA 8000C General protocols for pesticide residue identificationEPA 8081B Organochlorine pesticide detection by gas chromatographyEPA 8141B Organophosphorus pesticides in food matricesEPA 8151A Herbicide testing in soil and agricultural produceEPA 8151B LC-MS/MS testing of veterinary pesticide synergy effectsEPA 8270E Determination of semi-volatile pesticide residues in foodEPA 8321B Analysis of polar pesticides in animal tissues by HPLC-MSEPA 8325B Emerging pesticide residues in herbal medicinesEPA 8327 LC-MS analysis of pesticide degradation products in meatEPA 8330A Analysis of nitroaromatic pesticide residues in grainEU 2002/657/EC Validation of analytical methods for veterinary drug residuesEU 2005/34/EC Identification of residues in fresh meatEU 2009/128/EC Sustainable use of pesticides in food safety testingEU 2018/782 Residue control plan for animal-based food productsEU 2021/601 Monitoring of pesticide residues in organic foodEU 2022/617 Harmonization of veterinary residue testing protocolsEU 37/2010 Annex II Veterinary medicine residue validationEU 37/2010 Veterinary drug residue limits in foodstuffs of animal originEU 396/2005 Compliance Testing for Pesticide Residues in Fruits and VegetablesEU 396/2005 Harmonized limits for pesticide residues in food and feedEU 396/2005 Maximum residue limits of pesticides in agricultural products testingEU 625/2017 Compliance testing of veterinary drugs in aquacultureEU 744/2004 Residue control measures in aquacultureEU 96/23/EC Monitoring substances in live animals and animal productsEU SANTE/11813/2017 Sampling procedures for pesticide testingEU SANTE/12682/2019 Pesticide residues determination by QuEChERS methodEU SANTE/2020/12830 Confirmatory methods for residue analysisFAO/WHO Manual of Pesticide Residue Analysis in Agricultural CommoditiesISO 13395 Nitrite/nitrate detection in vegetables and fruitsISO 15662 Pesticide residue screening using modified QuEChERSISO 17094 Multiclass pesticide residue testing in oilseedsISO 17190 Detection of residues in fermented animal feedISO 18330 Pesticide and veterinary drug residue detection in herbsISO 18385 Measurement of pesticide residue cross-contaminationISO 1842 Analysis of pesticide residues in feed raw materialsISO 18512 Pesticide and antibiotic residues in animal dungISO 20418 Veterinary antibiotic residues in bovine serumISO 21010 Rapid screening for multi-class residues in animal tissueISO 21458 Screening of pesticide residues using multi-residue methodsISO 22855 Determination of pesticide degradation products in foodISO 22866 Determination of Spray Drift in Field Conditions for Pesticide ApplicationISO 22892 Analysis of persistent organic pollutants in livestockISO 23161 Screening of veterinary drug residues in eggsISO 23690 Determination of pesticide metabolites in animal feedISO 24662 Pesticide residue analysis in dried plant materialsISO 24687 Pesticide metabolite residue determination in poultryISO 25102 Multiresidue pesticide testing in spices and condimentsISO 6468 Pesticide residue analysis in water using liquid-liquid extractionJECFA Evaluation-Based Testing of Veterinary Drug Residues in Animal ProductsJECFA Pesticide residue risk evaluation for animal-derived productsJECFA Residue analysis of growth promoters in animal tissuesJECFA Residue evaluation of antibiotics in livestockJECFA Residue evaluation of veterinary drugs in cattle and poultryJECFA Residue limit setting for antimicrobials in livestockJECFA Risk assessment methodology for pesticide residue evaluationJECFA Risk-based residue evaluation for export commoditiesOECD TG 509 Residue Studies in Livestock for Veterinary Drugs DetectionSANCO/12495/2011 Method Validation for Pesticide Residue Analysis in FoodsVICH GL49 Risk Assessment Studies for Veterinary Medicinal Product Residues

Comprehensive Guide to ISO 15952 Pesticide Residue Testing in Animal Feedingstuffs Laboratory Testing Service Provided by Eurolab

ISO 15952 is an international standard that provides a framework for testing and monitoring pesticide residues in animal feedingstuffs. This standard is published by the International Organization for Standardization (ISO) and is widely adopted across the globe. The standard specifies the requirements for sampling, sample preparation, analysis, and reporting of pesticide residues in animal feedingstuffs.

Legal and Regulatory Framework

The use of pesticides in agriculture has raised concerns about their potential impact on human health and the environment. As a result, governments and regulatory bodies have established laws and regulations to ensure that pesticide residues are monitored and controlled. The European Unions (EU) Pesticide Regulation (EC) No 396/2005 is one such regulation that sets maximum residue limits (MRLs) for pesticides in food and animal feedingstuffs.

International and National Standards

ISO 15952 is based on several international and national standards, including:

  • ISO 15890: Animal feedingstuffs -- Sampling

  • ISO 15783: Animal feedingstuffs -- Sample preparation

  • EUs Pesticide Regulation (EC) No 396/2005

  • US EPAs Guidelines for Pesticide Residue Analysis

    • These standards provide a framework for testing and monitoring pesticide residues in animal feedingstuffs.

    Standard Development Organizations

    The International Organization for Standardization (ISO) is the primary standard development organization responsible for developing ISO 15952. Other organizations, such as ASTM International and EN, also contribute to the development of standards related to pesticide residue testing.

    Evolution of Standards

    Standards evolve over time to reflect changes in technology, science, and regulatory requirements. The development of new methods and techniques requires updates to existing standards to ensure that they remain relevant and effective.

    Specific Standard Numbers and Scope

    ISO 15952 is the primary standard for testing pesticide residues in animal feedingstuffs. Other related standards include:

  • ISO 15890: Animal feedingstuffs -- Sampling

  • ISO 15783: Animal feedingstuffs -- Sample preparation

    • These standards provide a framework for testing and monitoring pesticide residues in animal feedingstuffs.

    Standard Compliance Requirements

    Companies involved in the production, processing, and trade of animal feedingstuffs must comply with relevant standards and regulations. Failure to do so can result in non-compliance with regulatory requirements, which can lead to financial penalties, reputational damage, and loss of business.

  • Sampling methods: ISO 15890 provides guidance on sampling methods for animal feedingstuffs.

  • Sample preparation: ISO 15783 provides guidance on sample preparation techniques for animal feedingstuffs.

  • Analysis: ISO 15952 provides a framework for analyzing pesticide residues in animal feedingstuffs.

  • Reporting requirements: Results of pesticide residue testing must be reported in accordance with relevant standards and regulations.

  • Calibration and validation: Testing equipment and methods must be calibrated and validated to ensure accuracy and reliability.

    • ---

    Business and Technical Reasons for Conducting ISO 15952 Pesticide Residue Testing

    Pesticide residue testing is essential in ensuring that animal feedingstuffs are safe for consumption by humans. The use of pesticides can result in the presence of residues in animal feedingstuffs, which can have adverse effects on human health.

    Consequences of Not Performing this Test

    Failure to conduct pesticide residue testing can result in non-compliance with regulatory requirements, financial penalties, and reputational damage.

    Industries and Sectors that Require this Testing

    The following industries and sectors require ISO 15952 pesticide residue testing:

  • Animal feed manufacturers

  • Poultry and livestock producers

  • Crop growers and farmers

    • Risk Factors and Safety Implications

    Pesticide residues in animal feedingstuffs can have serious safety implications for human health, including:

  • Toxicity and carcinogenic effects

  • Endocrine disruption

  • Neurological damage

    • Quality Assurance and Quality Control Aspects

    ISO 15952 provides a framework for testing and monitoring pesticide residues in animal feedingstuffs. The standard requires that testing be conducted in accordance with good laboratory practice (GLP) principles, including:

  • Sampling methods: ISO 15890 provides guidance on sampling methods for animal feedingstuffs.

  • Sample preparation: ISO 15783 provides guidance on sample preparation techniques for animal feedingstuffs.

    • Contribution to Product Safety and Reliability

    ISO 15952 pesticide residue testing contributes to product safety and reliability by ensuring that animal feedingstuffs meet regulatory requirements for pesticide residues.

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    Detailed Step-by-Step Explanation of the Test

    The test involves the following steps:

    1. Sampling: A representative sample of animal feedingstuffs is collected from a production site or storage facility.

    2. Sample preparation: The sample is prepared for analysis in accordance with ISO 15783.

    3. Analysis: Pesticide residues are analyzed using a combination of methods, including chromatography and mass spectrometry.

    Sampling Methods

    ISO 15890 provides guidance on sampling methods for animal feedingstuffs. Sampling must be conducted in accordance with GLP principles to ensure that the sample is representative of the production site or storage facility.

    Sample Preparation Techniques

    ISO 15783 provides guidance on sample preparation techniques for animal feedingstuffs. Sample preparation involves preparing the sample for analysis, including homogenization and extraction.

    Analysis Methods

    ISO 15952 specifies a range of methods for analyzing pesticide residues in animal feedingstuffs. The most common methods include:

  • Chromatography: Gas chromatography (GC) or liquid chromatography (LC)

  • Mass spectrometry: Quadrupole mass spectrometry (QMS) or time-of-flight mass spectrometry (TOFMS)

    • Calibration and Validation

    Testing equipment and methods must be calibrated and validated to ensure accuracy and reliability. Calibration involves adjusting the testing equipment to ensure that it is functioning correctly, while validation involves demonstrating that the testing method can accurately detect pesticide residues.

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  • Quality control: The testing laboratory must have a quality control program in place to ensure that results are accurate and reliable.

  • Reporting requirements: Results of pesticide residue testing must be reported in accordance with relevant standards and regulations.

    • ---

    Conclusion

    ISO 15952 provides a framework for testing and monitoring pesticide residues in animal feedingstuffs. Companies involved in the production, processing, and trade of animal feedingstuffs must comply with relevant standards and regulations to ensure that their products meet regulatory requirements for pesticide residues.

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