EUROLAB
epa-5492-aldicarb-and-related-pesticide-testing-in-plant-tissue
Pesticide & Veterinary Drug Residues AOAC 2003.06 Chloramphenicol residue analysis in honeyAOAC 2004.08 Hormone residue detection in eggsAOAC 2006.03 Quantitation of residues in dairy productsAOAC 2007.01 Pesticide residue analysis in fruits and vegetables by LC-MS/MSAOAC 2008.05 Veterinary residue analysis in milk powderAOAC 2009.01 Pesticide residues in cocoa and chocolateAOAC 2010.01 Multiresidue analysis of pesticides in baby foodAOAC 2011.23 LC-MS/MS determination of sulfonamides in meatAOAC 2014.10 Tetracycline residues in fish and shellfish by ELISAAOAC 2015.06 Detection of pesticide residues in honey and bee productsAOAC 2016.04 Veterinary drug testing in poultry productsAOAC 2016.09 Veterinary drugs in seafood samplesAOAC 2017.02 Fluoroquinolone residue detection in beefAOAC 2017.09 Pesticide residues in citrus fruitsAOAC 2018.03 Veterinary drug residues in milk by LC-MS/MSAOAC 2018.09 Detection of macrolides in pork and beefAOAC 2019.02 Detection of β-lactam antibiotics in bovine milkAOAC 2020.04 LC-MS analysis of antiparasitics in sheep meatAOAC 2020.05 Multi-class pesticide screening in tea leavesAOAC 2021.06 Veterinary residues in dried meat productsAOAC 2022.01 Carbamate detection in vegetablesAOAC 2023.02 Veterinary drug screening in animal fatCAC/MRL 01 Maximum Residue Limits of Pesticides in Food Products TestingCodex CAC/MRL 1 Establishing pesticide MRLs in cereals and grainsCodex CXG 71-2009 Guidelines on residue monitoring programsCodex GL 56 Guidelines on Good Laboratory Practice for Pesticide Residue AnalysisCodex GL 56 Guidelines on performance criteria for methods of analysis for pesticidesCodex GL 71 Sampling for determination of pesticide residuesCodex GL 81 Good laboratory practices for pesticide residue testingCodex GL 90 Guideline levels for residues of veterinary drugs in foodCodex MRL Database Reference MRLs for pesticide-veterinary crossoverEPA 1657 Determination of pesticide metabolites in cropsEPA 3052 Determination of heavy metals in fertilizers and feed via acid digestionEPA 310.1 Herbicide detection in plant-based samplesEPA 314.1 Pesticide testing in animal urine samplesEPA 40 CFR Part 180 Analysis of Tolerances for Pesticide Chemical ResiduesEPA 5035A Sample preservation for volatile pesticide residue testingEPA 507 Pesticide analysis in drinking water and juicesEPA 535 Determination of chloroacetanilide herbicides in produceEPA 551.1 Determination of volatile pesticide residues in vegetablesEPA 6010D Trace metals in feed samples for pesticide contaminationEPA 608.3 Detection of pesticides in fat-rich animal tissuesEPA 8000C General protocols for pesticide residue identificationEPA 8081B Organochlorine pesticide detection by gas chromatographyEPA 8141B Organophosphorus pesticides in food matricesEPA 8151A Herbicide testing in soil and agricultural produceEPA 8151B LC-MS/MS testing of veterinary pesticide synergy effectsEPA 8270E Determination of semi-volatile pesticide residues in foodEPA 8321B Analysis of polar pesticides in animal tissues by HPLC-MSEPA 8325B Emerging pesticide residues in herbal medicinesEPA 8327 LC-MS analysis of pesticide degradation products in meatEPA 8330A Analysis of nitroaromatic pesticide residues in grainEU 2002/657/EC Validation of analytical methods for veterinary drug residuesEU 2005/34/EC Identification of residues in fresh meatEU 2009/128/EC Sustainable use of pesticides in food safety testingEU 2018/782 Residue control plan for animal-based food productsEU 2021/601 Monitoring of pesticide residues in organic foodEU 2022/617 Harmonization of veterinary residue testing protocolsEU 37/2010 Annex II Veterinary medicine residue validationEU 37/2010 Veterinary drug residue limits in foodstuffs of animal originEU 396/2005 Compliance Testing for Pesticide Residues in Fruits and VegetablesEU 396/2005 Harmonized limits for pesticide residues in food and feedEU 396/2005 Maximum residue limits of pesticides in agricultural products testingEU 625/2017 Compliance testing of veterinary drugs in aquacultureEU 744/2004 Residue control measures in aquacultureEU 96/23/EC Monitoring substances in live animals and animal productsEU SANTE/11813/2017 Sampling procedures for pesticide testingEU SANTE/12682/2019 Pesticide residues determination by QuEChERS methodEU SANTE/2020/12830 Confirmatory methods for residue analysisFAO/WHO Manual of Pesticide Residue Analysis in Agricultural CommoditiesISO 13395 Nitrite/nitrate detection in vegetables and fruitsISO 15662 Pesticide residue screening using modified QuEChERSISO 15952 Pesticide residue testing in animal feedingstuffsISO 17094 Multiclass pesticide residue testing in oilseedsISO 17190 Detection of residues in fermented animal feedISO 18330 Pesticide and veterinary drug residue detection in herbsISO 18385 Measurement of pesticide residue cross-contaminationISO 1842 Analysis of pesticide residues in feed raw materialsISO 18512 Pesticide and antibiotic residues in animal dungISO 20418 Veterinary antibiotic residues in bovine serumISO 21010 Rapid screening for multi-class residues in animal tissueISO 21458 Screening of pesticide residues using multi-residue methodsISO 22855 Determination of pesticide degradation products in foodISO 22866 Determination of Spray Drift in Field Conditions for Pesticide ApplicationISO 22892 Analysis of persistent organic pollutants in livestockISO 23161 Screening of veterinary drug residues in eggsISO 23690 Determination of pesticide metabolites in animal feedISO 24662 Pesticide residue analysis in dried plant materialsISO 24687 Pesticide metabolite residue determination in poultryISO 25102 Multiresidue pesticide testing in spices and condimentsISO 6468 Pesticide residue analysis in water using liquid-liquid extractionJECFA Evaluation-Based Testing of Veterinary Drug Residues in Animal ProductsJECFA Pesticide residue risk evaluation for animal-derived productsJECFA Residue analysis of growth promoters in animal tissuesJECFA Residue evaluation of antibiotics in livestockJECFA Residue evaluation of veterinary drugs in cattle and poultryJECFA Residue limit setting for antimicrobials in livestockJECFA Risk assessment methodology for pesticide residue evaluationJECFA Risk-based residue evaluation for export commoditiesOECD TG 509 Residue Studies in Livestock for Veterinary Drugs DetectionSANCO/12495/2011 Method Validation for Pesticide Residue Analysis in FoodsVICH GL49 Risk Assessment Studies for Veterinary Medicinal Product Residues

EPA 549.2 Aldicarb and Related Pesticide Testing in Plant Tissue: Eurolabs Laboratory Testing Service

The Environmental Protection Agency (EPA) has established a set of guidelines for the testing of pesticides in plant tissue, known as EPA 549.2 Aldicarb and related pesticide testing. This standard is designed to ensure that pesticide residues in plants are within safe levels for human consumption.

Overview of Relevant Standards

  • ISO/IEC 17025:2017 - General requirements for the competence of testing and calibration laboratories

  • ASTM E 1419-19 - Standard practice for sampling plant materials for residue analysis

  • EN 15662:2002 - Fertilizers - Sampling

  • TSE (Turkish Standards Institution) L 11/1.4 - Agricultural products - Sampling

    • These standards govern the testing of pesticides in plant tissue and ensure that laboratories follow strict protocols to produce accurate results.

    Legal and Regulatory Framework

    The use of pesticides is regulated by various government agencies, including the EPA, which sets limits for pesticide residues in plants. The FDA (Food and Drug Administration) also plays a role in ensuring that food products are safe for human consumption.

    International and National Standards

    International standards such as ISO 17025:2017 and ASTM E 1419-19 provide guidelines for laboratories to follow when testing pesticides in plant tissue. National standards, such as EN 15662:2002 and TSE L 11/1.4, may also apply depending on the country or region.

    Standard Development Organizations

    Standard development organizations, such as ISO (International Organization for Standardization) and ASTM (American Society for Testing and Materials), play a crucial role in developing and maintaining standards for laboratory testing.

    Evolution of Standards

    Standards evolve over time to reflect new technologies, methods, and research findings. This ensures that laboratories stay up-to-date with the latest techniques and protocols.

    Specific Standard Numbers and Scope

  • EPA 549.2: Aldicarb and related pesticide residues in plant tissue

  • ISO/IEC 17025:2017 - General requirements for the competence of testing and calibration laboratories (scope: laboratory testing)

  • ASTM E 1419-19 - Standard practice for sampling plant materials for residue analysis (scope: sampling)

    • Compliance Requirements

    Compliance with these standards is essential to ensure that laboratories produce accurate results. Failure to comply can result in inaccurate test results, which can have serious consequences.

    The testing of EPA 549.2 Aldicarb and related pesticide residues in plant tissue is required for several reasons:

    Business and Technical Reasons

  • To ensure that food products are safe for human consumption

  • To comply with government regulations

  • To maintain product quality and reputation

    • Consequences of Not Performing the Test

    Failure to perform this test can result in:

  • Inaccurate test results

  • Non-compliance with government regulations

  • Damage to product quality and reputation

    • Industries and Sectors

    This testing is required for various industries, including:

  • Food processing

  • Agriculture

  • Environmental monitoring

    • Risk Factors and Safety Implications

    Failure to perform this test can result in exposure to pesticide residues, which can have serious health implications.

    Quality Assurance and Quality Control Aspects

    To ensure accurate results, laboratories must follow strict quality assurance and quality control protocols, including:

  • Calibration of equipment

  • Validation of methods

  • Statistical analysis of data

    • Competitive Advantages

    Performing this test can provide several competitive advantages, including:

  • Increased customer confidence and trust

  • Improved product safety and reputation

  • Compliance with government regulations

    • Cost-Benefit Analysis

    The benefits of performing this test far outweigh the costs.

    The testing of EPA 549.2 Aldicarb and related pesticide residues in plant tissue involves several steps:

    Testing Equipment and Instruments

  • Gas chromatograph

  • Mass spectrometer

  • Sample preparation equipment

    • Testing Environment Requirements

  • Temperature: 20C 5C

  • Humidity: 50 10

  • Pressure: atmospheric pressure

    • Sample Preparation Procedures

    Samples are prepared using a combination of solvent extraction and clean-up techniques.

    Testing Parameters and Conditions

  • Extraction solvent: acetonitrile

  • Clean-up procedure: solid-phase extraction (SPE)

  • Chromatographic conditions: temperature, column type, and flow rate

    • Measurement and Analysis Methods

    Results are measured using a combination of gas chromatography and mass spectrometry.

    Calibration and Validation Procedures

    Equipment is calibrated regularly to ensure accuracy. Methods are validated using certified reference materials.

    Measuring Pesticide Residues in Plant Tissue

    To determine pesticide residues in plant tissue, laboratories use a combination of sampling, extraction, clean-up, and analysis techniques.

    1. Sampling: Samples are collected from the field or processing facility.

    2. Extraction: Samples are extracted using an appropriate solvent (e.g., acetonitrile).

    3. Clean-up: The extract is cleaned up using a solid-phase extraction (SPE) cartridge.

    4. Analysis: The clean-up extract is analyzed by gas chromatography-mass spectrometry (GC-MS).

    Measuring Pesticide Residues in Plant Tissue

    To determine pesticide residues in plant tissue, laboratories use a combination of sampling, extraction, clean-up, and analysis techniques.

    1. Sampling: Samples are collected from the field or processing facility.

    2. Extraction: Samples are extracted using an appropriate solvent (e.g., acetonitrile).

    3. Clean-up: The extract is cleaned up using a solid-phase extraction (SPE) cartridge.

    4. Analysis: The clean-up extract is analyzed by gas chromatography-mass spectrometry (GC-MS).

    Measuring Pesticide Residues in Plant Tissue

    To determine pesticide residues in plant tissue, laboratories use a combination of sampling, extraction, clean-up, and analysis techniques.

    1. Sampling: Samples are collected from the field or processing facility.

    2. Extraction: Samples are extracted using an appropriate solvent (e.g., acetonitrile).

    3. Clean-up: The extract is cleaned up using a solid-phase extraction (SPE) cartridge.

    4. Analysis: The clean-up extract is analyzed by gas chromatography-mass spectrometry (GC-MS).

    Quality Assurance and Quality Control

    Laboratories must follow strict quality assurance and quality control protocols to ensure accurate results.

    1. Calibration of equipment

    2. Validation of methods

    3. Statistical analysis of data

    Certification and Accreditation

    Laboratories must be certified by a recognized certification body (e.g., ISO/IEC 17025:2017) to demonstrate competence in testing pesticides in plant tissue.

    Accredited Laboratory Services for EPA 549.2 Aldicarb Testing

    Eurolab is an accredited laboratory that provides reliable and accurate results for the testing of EPA 549.2 Aldicarb and related pesticide residues in plant tissue.

    Need help or have a question?
    Contact us for prompt assistance and solutions.

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