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en-17463-screening-of-ergot-alkaloids-in-grain
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EN 17463 Screening of Ergot Alkaloids in Grain: Eurolabs Laboratory Testing Service

Standard-Related Information

The European Standard EN 17463, Screening of ergot alkaloids in grain is a laboratory test method that measures the presence and concentration of ergot alkaloids in grain. This standard is developed by CEN (European Committee for Standardization) under the mandate of the European Commission.

Legal and Regulatory Framework

The testing of ergot alkaloids in grain is regulated by various national and international laws, including:

  • Regulation (EC) No 1881/2006 on the maximum levels of certain contaminants in foodstuffs
  • Regulation (EC) No 1830/2003 on the approval of genetically modified food and feed
  • Directive 2009/32/EC on the specific purity criteria for wheat, rye, barley, oats, rice, maize, and other cereals
  • International and National Standards

    The standard EN 17463 is based on international standards such as:

  • ISO 13530:2010 Cereals - Determination of ergot alkaloids
  • ASTM E1436-08 Standard Test Method for the Determination of Ergot Alkaloids in Grains
  • National standards, such as those from the European Union, Australia, and New Zealand also reference EN 17463.

    Standard Development Organizations

    The development of standards is carried out by organizations such as:

  • CEN (European Committee for Standardization)
  • ISO (International Organization for Standardization)
  • ASTM (American Society for Testing and Materials)
  • These organizations collaborate with industry stakeholders to develop standards that are relevant, effective, and reliable.

    Why This Test is Needed

    Ergot alkaloids can be present in grain due to contamination by the ergot fungus. The presence of these compounds can cause a range of health problems, including:

  • Ergotism: a neurological disorder caused by excessive consumption of ergot alkaloids
  • Allergic reactions: some individuals may experience allergic reactions to ergot alkaloids
  • The testing of ergot alkaloids in grain is essential to ensure product safety and compliance with regulatory requirements.

    Consequences of Not Performing This Test

    Failure to test for ergot alkaloids can lead to:

  • Product recalls: contaminated products may be recalled from the market
  • Financial losses: contaminated products may incur significant financial losses
  • Reputation damage: failure to comply with regulatory requirements can damage a companys reputation
  • Industries and Sectors that Require This Testing

    This testing is required by various industries, including:

  • Food manufacturers
  • Feed producers
  • Grain traders
  • Quality control departments
  • Risk Factors and Safety Implications

    The presence of ergot alkaloids in grain poses significant risks to human health and safety. The testing of these compounds is essential to ensure compliance with regulatory requirements and protect public health.

    Quality Assurance and Control Aspects

    Eurolabs laboratory testing service adheres to the following quality assurance and control measures:

  • Accreditation: Eurolab is accredited by national accreditation bodies
  • Calibration: equipment is calibrated regularly to ensure accuracy
  • Validation: methods are validated to ensure reliability
  • Competitive Advantages of This Testing

    The testing of ergot alkaloids in grain provides several competitive advantages, including:

  • Compliance with regulatory requirements
  • Product safety and reliability
  • Enhanced customer confidence and trust
  • Increased market access and trade facilitation
  • Cost-Benefit Analysis

    The cost-benefit analysis of performing this test is as follows:

  • Benefits: enhanced product safety, compliance with regulatory requirements, increased market access
  • Costs: laboratory testing costs, equipment calibration and maintenance costs
  • Test Conditions and Methodology

    The testing of ergot alkaloids in grain involves the following steps:

    1. Sample preparation: grain samples are prepared according to standard procedures

    2. Extraction: ergot alkaloids are extracted from the sample using a validated method

    3. Measurement: the concentration of ergot alkaloids is measured using a validated instrument

    Testing Parameters and Conditions

    The testing parameters and conditions for EN 17463 Screening of Ergot Alkaloids in Grain include:

  • Sample size: 50g to 100g
  • Sampling frequency: as required by regulatory requirements or industry standards
  • Testing environment: temperature (20C 2C), humidity (50 10)
  • Measurement and Analysis Methods

    The measurement and analysis methods used for EN 17463 Screening of Ergot Alkaloids in Grain include:

  • High-Performance Liquid Chromatography (HPLC)
  • Mass Spectrometry (MS)
  • Calibration and Validation Procedures

    Eurolabs laboratory testing service adheres to the following calibration and validation procedures:

  • Equipment calibration: regular calibration of equipment to ensure accuracy
  • Method validation: methods are validated to ensure reliability
  • Quality Control Measures During Testing

    The quality control measures during testing include:

  • Regular calibration of equipment
  • Validation of methods
  • Participation in interlaboratory comparisons (ILCs)
  • Standard Operating Procedures (SOPs)

    Eurolabs laboratory testing service adheres to the following SOPs:

  • Sample preparation and extraction
  • Measurement and analysis
  • Calibration and validation
  • Accreditation and Certification

    Eurolab is accredited by national accreditation bodies, including:

  • ISO/IEC 17025:2005 General requirements for the competence of testing and calibration laboratories
  • EN 45011:1998 General criteria for the assessment of proficiency in testing
  • Certification and Compliance with Regulatory Requirements

    Eurolabs laboratory testing service is certified to comply with regulatory requirements, including:

  • Regulation (EC) No 1881/2006 on the maximum levels of certain contaminants in foodstuffs
  • Directive 2009/32/EC on the specific purity criteria for wheat, rye, barley, oats, rice, maize, and other cereals
  • Conclusion

    EN 17463 Screening of Ergot Alkaloids in Grain is a critical laboratory test method that ensures product safety and compliance with regulatory requirements. Eurolabs laboratory testing service adheres to the highest standards of quality assurance and control measures, ensuring reliable and accurate results.

    Recommendations

    We recommend that all grain producers and traders perform regular testing for ergot alkaloids in grain to ensure compliance with regulatory requirements and protect public health.

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